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A solution of amine salt 136 (700 mg, 1.50 mmol) andmethyl3,5-diamino-6-chloropyrazine-2-carbonylcarbamimidothioate (13, 880 mg, 2.26 mmol) in EtOH (30 mL) was charged with DIPEA (2.15 mL, 12.03 mmol) at room temperature
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10.1016/j.jbc.2021.100929
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